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GCMS analysis log for sample AD31024

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

NYC-WTC_000017494–000017513

Folder label: “GCMS X 12/20/01 A 1/8/02

Page image
Scanned page image, NYC-WTC_000017502
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document Library Search Compound Report . °°" pata File : C:\HPCHEM\1\DATA\JANO802\31024.D Vial: 16 Acq On : 9 dan 2002 3:58 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eeVeetrrrrcrrterer fs erererrrrrreertrrrrrt irri itt itt t itt tt titi rrr t ry Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 6 R.T. | EstCone Area Relative to ISTD R.T. 11.00 1.38 ug/1 350951 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cAs# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 86 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 _4..2-0x0-4-pheny1-6-(4-chlorophenyl) -1 282 C16H11CIN20___000000-00-0 8 Abundance ‘Sean 648 (10.906 min}: 31024.) vy | /% 281-00 100.008 | | | 5000} | i | | 8 133 183 297 249 265 |) | 10.60 10180 11:00 41:20 11:40 | 4850 "P99 103 119 | 147 163.17 221 235 49 26 Sao RE CILEC mz->__40__ 6080 400120 140 _160_180_200 220 240 260 _280 i) | Abundance #73646: Gydlotetvasiloxane, Sctamethy- 7 2 | | | | LA | ia | | | -t0!60 “to'so ‘11100 11120 11.40 | | |m/z 283.00 17.03 45_so 78 133 1712207 ay \ miz-> 40-6080 100-120 140160 180 200 220 240 260 280 Abundance FEST: 6 fohianze proreinin | 281 | 10.60 ‘10.80 11:00 11:20 11.40 5000: [m/z 192.90 11.88: | 102 118 +189 204 "250264 | | svz> “40” 6'60 "400420140 "180 "480200 220" 240 260 280 | | ‘Abundance +¥#20643: Benzene, 1-pheny/-4-(2-cyano-2-phenyletheny/) | 4 | 21 10.60__10.80_11.00_11.20_ 11.40. m/z 133.00 11.79! 253 126 3 mo | miz-> 40-60-80 100 120 140 160 180 200 220 240 260 280 | 10.60 10.80 11.00 11.20 1140 31024.D GCMS0103.M Wed Jan 09 12:14:50 2002 Page 2 NYC-WTC_000017502

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NYC-WTC_000017502Source: NYC Law Department, mirrored locally

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Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

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NYC-WTC_000017344

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