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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017280
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document Library Search Compound Report . . ‘Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 Acq On : 9 Jan 2002 4:56 am Operator: 209 GALOS Sample : goms scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eTeotrrrrerr teres Sr errer: frre rerrrrr rr rrr rte rier ttt rrr rit rrr tr Ts Peak Number 9 N-(Trifluoracetyl)-0,0',O"-tri Concentration Rank 5 R.T. EstCone Area Relative to ISTD R.T. 22.64 2.31 ug/ 776323 Phenanthrene-d10 24.81 Hit# of 5 mtative ID MW MolForm cas# Qual 1 N-(Triflugfacetyl)-0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 2 Benzoic gcid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 38 3 Benzenegthanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 N-(Trifluoroacetyl) -N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 35 Abundance ‘Scan 1817 (22.640 min): 30605. m/z 72.95 100.00% | s00 | 45 | "yr | at 22402260 22.80 23.00 | Ba hr e a h 249. - m/z 147.00 26.528) sal 50 100 __150 200 250 300 350 400 450 500 550 bundancs #58807: N-(Trifluoracetyi}-O,0" O"-tris(trimethyisiiyepin | ' i 355 5000: ‘22140 22160 22.80 23.00 | m7 m/z 355.05 24.94% 140 leer peti et rereperts 498 ra 50 100 _ _150 200 250 300 350 400 450 500 550 Ring SB a 51296; Benzois ued, DE-bisfeimathy Sivan. trmet * 355 | ‘22:40 22.60 22160 73.00 | $000 | m/z 221.05 17.67! | 47 L 208 237 gh = 50. 100 _150 200 250 300 “ 460 450 500 550. ‘Rounders ‘#74706: Betzeneethanamine, N-{(pentafluorophenyi}methyiene] 355 2240 22.60 22.80 23.00 m/z 281.00 13.72 | S000: i | uid 208251 281 386458 a | iz» "60.100" 150200250 300360400450 600 580 22:40. 22.60 228023100 30605.D GCMS0103.M Tue Jan 15 09:31:34 2002 Page 9 NYC-WTC_000017280

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NYC-WTC_000017280Source: NYC Law Department, mirrored locally

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