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Document / 14 pages

GCMS scan data for sample AD30604

Machine-extracted title · confidence 90%

Instrument output from a gas chromatography-mass spectrometry scan of sample AD30604 conducted on January 18, 2002.

NYC-WTC_000017157–000017170

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017159
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NYC 9/11 Public Portal Document a: Quantitation Report (QT Reviewed) ir Data File : C:\HPCHEM\1\DATA\DEC2701\30604.D Vial: 34 Acq On : 28 Dec 2001 10:13 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 14:13 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.67 152 . 837829 20.00 ug/l -0.02 10) Naphthalene-ds 15.28 136 3183437 20.00 ug/l -0.02 17) Acenaphthene-d10 20.56 164 1560455 20.00 ug/l -0.01 29) Phenanthrene-d10 24,99 188 2295806m 20.00 ug/l 0.00 38) Chrysene-d12 33.02 240 1429925 20.00 ug/l -0.01 44) Perylene-d12 37.11 264 824665 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 30.06 235 87981 3.49 ug/mL 0.00 Spiked Amount 5.000 Recovery = 69.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.17 74 432 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0) N.D. 4) 1,3-Dichlorobenzene 0.00 146 0) N.D. 5) 1,4-Dichlorobenzene 0.00 146 0) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0) N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 C) N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 13.1177 118 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chlorcethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 661 N.D. 16) Hexachlorobutadiene 0.00 225 0) N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 0.00 162 ° N.D. 20) Dimethylphthalate 0.00 163 C) N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 C) N.D. 23) Acenaphthene 0.00 153 0) N.D. 24) 2,4-Dinitrotoluene 21.41 165 102 N.D. 25) Diethylphthalate 22.13 149 425 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 ° N.D. (#) = qualifier out of range (m) = manual integration 30604.D GCMS1126.M Mon Dec 31 14:13:28 2001 Page 1 NYC-WTC_000017159

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NYC-WTC_000017159Source: NYC Law Department, mirrored locally

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