NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GCMS analysis results for sample AD30633, Jan 2002
Machine-extracted title · confidence 95%Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
NYC-WTC_000017210–000017232Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 16:11 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.68 152 1085459 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 4194966 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 2049830 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 3084102 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1868446 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1074128 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.06 235 125512 3.70 ug/mL 0.00 Spiked Amount 5.000 Recovery = 74.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.13 74 1258 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.53 77 100 N.D. 12) Isophorone 14.30 82 185 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1860 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.28 163 1503 N.D. 21) 2,6-Dinitrotoluene 20.27 165 704 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.30 165 225 N.D. 25) Diethylphthalate 22.12 149 2100 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 30633.D GCMS1126.M Mon Dec 31 13:51:04 2001 Page 1
NYC-WTC_000017212
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NYC-WTC_000017212Source: NYC Law Department, mirrored locally
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Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
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