GCMS analysis results, sample AD30602, January 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2701\30602.D Vial: 30 Acq On : 28 Dec 2001 6:18 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 14:09 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.68 152 1114759 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 4287612 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 2130486 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 3150639m 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1934453 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 1102096 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 128337 3.71 ug/mL 0.00 Spiked Amount 5.000 Recovery = 74.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 325 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.46 77 176 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1449 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.28 163 596 N.D. 21) 2,6-Dinitrotoluene 20.28 165 129 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.32 165 221 N.D. 25) Diethylphthalate 22.13 149 1521 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30602.D GCMS1126.M Mon Dec 31 14:09:23 2001 Page 1

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