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GCMS analysis results, sample AD30602, January 2002

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Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.

NYC-WTC_000017246–000017264

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2701\30602.D Vial: 30 Acq On : 28 Dec 2001 6:18 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 14:09 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.99 178 1696 N.D. 34) Anthracene 24.99 178 1696 N.D. 35) Di-n-butylphthalate 27.02 149 24401 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.71 149 2003 N.D. 41) Benzo(a)anthracene 33.02 228 4976 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 5972 N.D. 43) Chrysene 33.02 228 4976 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.12 252 4596 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g, h, i) perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30602.D GCMS1126.M Mon Dec 31 14:09:26 2001 Page 2

NYC-WTC_000017249

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NYC-WTC_000017249Source: NYC Law Department, mirrored locally

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