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GCMS sample analysis results, Jan 2002

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Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30085 conducted on January 9, 2002.

NYC-WTC_000019061–000019069

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2101\30085.D Vial: 7 Acq On : 22 Dec 2001 12:42 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 22 13:31 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.05 178 270 N.D. 3 4) Anthracene 25.05 178 270 N.D. 35) Di-n-butylphthalate 27.00 149 17074 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 3658 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 8789 N.D. 43) Chrysene 33.02 228 3658 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.11 252 3514 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30085.D GCMS1126.M Thu Dec 27 09:57:19 2001 Page 2

NYC-WTC_000019064

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NYC-WTC_000019064Source: NYC Law Department, mirrored locally

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