NYC-WTC_000016726
GCMS analysis of environmental sample AD30112 conducted January 9, 2002.
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GCMS sample analysis results, Jan 2002
Machine-extracted title · confidence 90%Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30313 conducted on January 9, 2002.
NYC-WTC_000019100–000019110Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2101\30313.D Vial: 14 Acq On : 22 Dec 2001 7:31 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 22 20:20 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 923828 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3467062 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1729228 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2448737 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1242566 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 753730 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 123314 3.48 ug/mL -0.02 Spiked Amount 5.000 Recovery = 69.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1732 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.18 165 101 N.D. 25) Diethylphthalate 22.10 149 11219 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 30313.D GCMS1126.M Thu Dec 27 10:02:12 2001 Page 1
NYC-WTC_000019102
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