GCMS sample analysis results, Jan 2002

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Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30314 conducted on January 9, 2002.

NYC-WTC_000019121–000019129

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2101\30314.D Vial: 5 Acq On : 22 Dec 2001 10:45 am Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 22 11:34 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 962336 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3687432 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1795677 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2642796 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1428897 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 897389 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.05 235 147106 3.85 ug/mL -0.02 Spiked Amount 5.000 Recovery = 77.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.19 74 756 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.71 146 174 N.D. 5) 1,4-Dichlorobenzene 11.71 146 174 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1951 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 20.57 153 112 N.D. 24) 2,4-Dinitrotoluene 21.07 165 607 N.D. 25) Diethylphthalate 22.11 149 903 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30314.D GCMS1126.M Thu Dec 27 09:56:00 2001 Page 1

NYC-WTC_000019123

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