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GCMS analysis results for sample AD30351, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.

NYC-WTC_000017833–000017853

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2 701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 12:16 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 900008 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 3487908 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1780113 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2559658m 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1597359 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 977099 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 186017 5.02 ug/mL -0.01 Spiked Amount 5.000 Recovery = 100.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. • 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.78 77 103 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1516 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.27 163 888 N.D. 21) 2,6-Dinitrotoluene 20.28 165 409 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.33 165 178 N.D. 25) Diethylphthalate 22.14 149 2010 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30351.D GCMS1126.M Mon Dec 31 12:18:33 2001 Page 1

NYC-WTC_000017835

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NYC-WTC_000017835Source: NYC Law Department, mirrored locally

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