NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2 701\30256.D Vial: 17
Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS
Sample : GC/MS SCAN Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Dec 29 15:35 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 875525 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 3364736 20.00 ug/1 -0.02
17) Acenaphthene-dl0 20.56 164 1703327 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.99 188 2555989 20.00 ug/1 0.00
38) Chrysene-dl2 33.03 240 1527691 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 878996 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.06 235 101644 3.62 ug/mL 0.00
Spiked Amount 5.000 Recovery = 72.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.20 74 223 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.35 128 1450 N.D.'
16) Hexachiorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.51 162 186 N.D.
20) Dimethylphthalate 20.28 163 978 N.D.
21) 2,6-Dinitrotoluene 20.28 165 407 N.D.
22) Acenaphthylene 20.29 152 174 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.20 165 869 N.D.
25) Diethylphthalate 22.04 149 387 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30256.D GCMS1126.M Mon Dec 31 11:46:43 2001 Page 1
NYC-WTC_000019132
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