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GCMS analysis report for sample AD30009, January 2002

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Laboratory GCMS analysis report for sample AD30009 conducted on January 9, 2002, by analyst DLV.

NYC-WTC_000016816–000016825

Folder label: “GCMS X 12/12/01 A 12/20/01

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NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\DEC2101\30009.D Vial: 25 Acq On : 21 Dec 2001 2:14. pm Operator: 209 GALOS Sample : gc/ms scan 12/12 a Inst : GC/MS 209 Mise 3 Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 27 8:52 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T, QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 1015152 20.00 ug/l -0.02 10) Naphthalene-ds 15.28 136 3909190 20.00 ug/l -0.03 17) Acenaphthene-d10 20.55 164 1928176 20.00 ug/l -0.02 29) Phenanthrene-dio 24.98 188 2764316m 20.00 ug/l -0.01 38) Chrysene-d12 33.01 240 1744260 20.00 ug/l -0.02 44) Perylene-di2 37.11 264 1164632 20.00 ug/l -0.01 System Monitoring Compounds 37) 2,4-DDD 30.06 235 142827 3.57 ug/mL -0.01 Spiked Amount 5.000 Recovery = 71.40% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.34 74 259 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 ° N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.3777 122 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 ° N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.34 128 1327 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0) N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 ° N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 ° N.D. 24) 2,4-Dinitrotoluene 21.23 165 178 N.D. 25) Diethylphthalate 22.11 149 1102 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0) N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 17 oO N.D. (#) = qualifier out of range (m) = manual integration 30009.D GCMS1126.M Mon Dec 31 12:34:09 2001 Page 1 NYC-WTC_000016818

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NYC-WTC_000016818Source: NYC Law Department, mirrored locally

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