NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis log for sample AD30603
Machine-extracted title · confidence 95%Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.
NYC-WTC_000017233–000017245Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document .¢ Quantitation Report (QT Reviewed) «. Data File : C:\HPCHEM\1\DATA\DEC2701\30603.D Vial: 31 Acq On : 28 Dec 2001 7:17 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 20:06 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 1310666 20.00 ug/l -0.02 10) Naphthalene-d8 15.28 136 5074347 20.00 ug/l -0.03 17) Acenaphthene-d10 20.57 164 2404300 20.00 ug/1 0.00 29) Phenanthrene-d10 24.98 188 3821521 20.00 ug/l 0.00 38) Chrysene-di2 33.02 240 2412118 20.00 ug/1 0.00 44) Perylene-d12 37.12 264 1417402 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 30.06 235 184771 4.40 ug/mL -0.01 Spiked Amount 5.000 Recovery = 88.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.30 74 282 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0) N.D. 5) 1,4-Dichlorobenzene 0.00 146 C) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0) N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 to) N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 ) N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 13.59 82 391 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 te) N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.33 128 2146 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.28 163 287 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 oO N.D. 24) 2,4-Dinitrotoluene 21.28 165 322 N.D. 25) Diethylphthalate 22.10 149 1701 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0) N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 i) N.D. (#) = qualifier out of range (m) = manual integration 30603.D GCMS1126.M Mon Dec 31 14:11:26 2001 Page 1 NYC-WTC_000017235
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NYC-WTC_000017235Source: NYC Law Department, mirrored locally
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Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.
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NYC-WTC_000036931
GCMS analysis report for sample AD29565 listing unknown compounds and surrogate recovery data from January 22, 2002.
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