GCMS analysis report for sample AD30114, January 2002

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Laboratory GCMS analysis report for sample AD30114 conducted on January 9, 2002, by analyst DLV.

NYC-WTC_000016863–000016871

Folder label: “GCMS X 12/12/01 A 12/20/01”

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NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\DEC1901\30114.D Vial: 18 Acq On : 20 Dec 2001 6:03 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 12:26 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 795327 20.00 ug/l -0.02 10) Naphthalene-ds 15.27 136 3005680 20.00 ug/l -0.03 17) Acenaphthene-di0 20.55 164 1486302 20.00 ug/l -0.02 29) Phenanthrene-d10 24.98 188 2145193m 20.00-ug/l -0.01 38) Chrysene-di2 33.01 240 1309338 20.00 ug/l -0.02 44) Perylene-di2 37.10 264 797925 20.00 ug/l = -0.01 System Monitoring Compounds 37) 2,4-DDD 30.05 235 109781 3.54 ug/mL -0.02 Spiked Amount 5.000 Recovery = 70.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.23 74 740 N.D. 3) bis(2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 ° N.D. 5) 1,4-Dichlorobenzene 0.00 146 0) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 0.00 77 ° N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.33 128 979 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 ° N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 ° N.D. 22) Acenaphthylene 0.00 152 ° N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.13 165 176 N.D. 25) Diethylphthalate 22.13 149 285 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0) N.D. 27) Fluorene 0.00 166 C) N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 30114.D GCMS1126.M Mon Dec 31 12:27:02 2001 Page 1 NYC-WTC_000016865

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NYC-WTC_000016865Source: NYC Law Department, mirrored locally

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