GCMS analysis results for sample AD27823, Jan 2002

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Laboratory report documenting GCMS analysis of environmental sample AD27823 conducted on January 3, 2002.

NYC-WTC_000033662–000033673

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1901\27823.D Vial: 31 Acq On : 19 Dec 2001 8:32 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst . : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 19 21:21 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.66 152 736907 20.00 ug/1 -0.04 10) Naphthalene-d8 15.28 136 2805814 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1378974 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.97 188 2050212 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1330149 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 859057 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 12) Isophorone 12.88 0.00 77 82 (101 0 N.D. N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 N.D. 15) Naphthalene 15.33 128 201/ N.D. 16) Hexachlorobutadiene 0.00 225 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.96 165 432 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 27823.D GCMS1126.M Mon Dec 31 11:14:13 2001 Page 1

NYC-WTC_000033664

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