GCMS analysis results for sample AD30109, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1901\30109.D Vial: 20 Acq On : 20 Dec 2001 8:01 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 12:21 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.67 152 889541 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3444253 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1701289 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2557806m 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1734289 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 1229102 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.06 235 140039 3.78 ug/mL -0.01 Spiked Amount 5.000 Recovery = 75.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 385 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Di chlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1316 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.14 165 103 N.D. 25) Diethylphthalate 22.11 149 1116 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30109.D GCMS1126.M Mon Dec 31 12:22:21 2001 Page 1

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