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GCMS unknowns analysis report for sample AD31346, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31346 using GCMS on February 11, 2002.

NYC-WTC_000017016–000017025

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000017024
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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0902\31346.D Vial: 12 Acq On : 11 Jan 2002 2:18 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE ISOS ESSE OIS I IESE EISISISI IIIS ITO ISUOISIODI TOO IOEI ISI IOS Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. | EstCone Area Relative to ISTD R.T. 14.17 0.30 ug/l 75480 Naphthalene-d8 15.12 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Cyclopentasilgkane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 N-(Trifluorodcetyl) -N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 35 3 Phenethylgnfine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 32 _4 11H-DiberZo [b, E] [1,4]diazepin-11-on 267 C16H17N30 __ 013450-73-2 27 = Scan 994 (14.479 min): 31346.D G) “Tm/z 73.90 100.00 5000. 7 | ar 2385 | | 45 193 43.80 14.00 14.20 14.40 14.60 foe 1 eee oe m/z 267.00 38.65 miz>___80 100 __150__200__250 _300 350 _400__450 500 __ 50. | ‘Abundance #51266: Cyclopentasiloxane, decamethyk ass . 5000: 267 — - 13.80 14.00 14.20 14.40 14.60 m/z 355.0; 32.67 207 323, a | 385 13.80 14.00 14.20 14.40 14.60 5000 m/z 356.0, 12.78% - 147__ 193 267 598 miz-> ___§0___100 _150_ 200 __250___300 350 400 __450___500__ 550 ‘Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-trs(trimethyis | 43.80 14.00 14.20 14.40 14.60 m/z 268.00 10.59 5000: 355 . “a Fj 147 _ 199 267 204 ma _80_100_ 180_ 200250 300.380.400.450. 500_ 80 | 13.80 14.00 14.20 1440 14.60 31346.D GCMS0103.M Tue Feb 05 16:58:35 2002 Page 2 NYC-WTC_000017024

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NYC-WTC_000017024Source: NYC Law Department, mirrored locally

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