GCMS sample AE12761 results, June 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\060602\12762.D Vial: 8 Acq On 6 Jun 2002 5:00 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 11 3,5-Ethanoquinolin-10-one, . Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

5.36 0.32 ug/L 227091 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 3,5-Ethanoquinolin-10-one, decah... 207 C13H21NO 021041-42-9/9 2 Diethylpropion Hydrochloride 205 C13H19NO 000134-80 9 3 1,2-Ethanedithiol 94 C2H6S2 000540-63-6 9 4 1,2-Ethanedithiol 94 C2H6S2 000540/63-6 9 Abundance Scan 388 (5.359 min): 12762.D (-385) (-) m/z 206.90 6 100.00% 207 47

5000 35 87 5.00 5.20 5.40 5.60 5.80

n/z-> 0- mrHHI—. .......... Il.......... .......................... 1’111191111111111111012111911115111110110131311111111112111113303221177 p-rrr 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 m/z 47.00 74.15% Abundance #84800:3,5-Ethanoquinolin-10-one, decahydro-1,7-dimethyl-... 164 207

96 5000 44 5.00 5.20 5.40 5.60 5.80 70 150 192 m/z 51.00 55.42% 27 57 82 108 122 136 179 "... _ 0------- mH " • i ■ TT ■p-TTT iz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #12303: Diethylpropion Hydrochloride 47 100

5 00 5.20 5.40 5.60 5.80 5000 63 m/z 49.10 37.15%

i , 205 0-’ 1-131113 TOuDmT niz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #111015: 1,2-Ethanedithiol 47 60 94 5.00 5.20 5.40 5.60 5.80 27 m/z 208.00 29.57% 5000

mfe-> 0 4 47f 'I'11" • ■ । ।

20 30 40 50 60 70 80 90 100110120130140150160170180190200210 " i' • ■ ■ । ■ i ■ ■ “ ।“ i" ■ ■ i “ ■' ।1 “ • । "11 ■ ■"

5.00 5,20 5.40 5.60 5.80

12762.D 060302.M Mon Jun 10 10:26:45 2002 Page 14

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