GCMS analysis results, sample AE12288, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12288.D Vial: 7 Acq On : 29 May 2002 2:58 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan '= Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 4 3-Aza-5-hexylene-l-ol, N,N-... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.81 0.94 ug/L 669249 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Aza-5-hexylene-l-ol, N,N-dimet... 173 C8H17N202 1000124-82-7 4 2 Ethanethiol, 2-amino-, hydrochio... 113 C2H8C1NS 000156-57-0 4 3 2-Propanethiol 76 C3H8S 000075-33-2 2 4 Propanoy1 chloride 92 C3H5C1O 000079-03-8 2 Abundance Scan 125 (3.814 min): 12288.D (-124) (-) m/z 48.00 100.00% 48

5000 38 87 wMMMMMusww* 58 i 1 ■ ■ ■ i 1 ' 3.40 3.60 3.80 4.00 4.20 O+ • "i' “ 'i" " i1 “ Hr i ■1 ‘11 ■ ■ ■ • i ■ ■ 11’011151——09001—3B70000110300E310t0T m/z 38.10 75.14% Wz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #3342:3-Aza-5-hexylene-1-ol, N,N-dimethyl-, carbaminate e... 42 58 5000 I 1 • ■ ■ I 3.40 3.60 3.80 4.00 4.20 m/z 42.00 58.47% 71 84

m/z-> Abundance Of 15944 T . .if,|........... 96 106115 129 144 157165173 I ■ rl’t’hrl ,HT|.... pr.11-. r rT’ . 1,! 11,! |. I rr.-. 11.| . 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #715: Ethanethiol, 2-amino-, hydrochloride 30 N . 3.40 3.60 3.80 4.00 4.20 5000 m/z 87.00 57.10% 38 47 59 77 15 - 0- I ■i■■।11" “ i ■ ■ ■■i “ ■ ■ i ■ ■ ‘ ■ i “ i'11111111111" r711111111" n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #109210:2-Propanethiol 43 3.40 3.60 3.80 4.00 4.20 ^m/z^ 27 5000 76 61 15 35, 0 —r l r -1' i"1 ■ i ■" ■ i ■"11" ‘ ■ i" “ i •' ■' i “ " i" " i' “ ‘ i" " i' ■ m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 3.40 3.60 3.80 4.00 4.20

12288.D 052202.M Mon Jun 03 09:37:03 2002 Page 7

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