GCMS reference analysis results for volatile organics, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\060702\12735.D Vial: 11 Acq On 7 Jun 2002 4:43 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Ethanamine, N-ethyl-N-[(eth... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.07 1.28 ug/L 893739 1,4-dichlorobenzene-d4 9.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanamine, N-ethyl-N-[(ethylthi... 147 C7H17NS 003492-79-3 9/ 2 Propanal, 2-methyl-2-(methylsulf... 149 C5H11NO2S 007635-32-7 9 3 Dianhydromannitol 146 C6H10O4 1000127-66-7 9 4 1,3-Dioxol-2-one 86 C3H203 000872-3676 7 Abundance Scan 169 (4.072 min): 12735.D (-167) (-) m/z 49.10 100.00% 49 86

41 5000 58 * ' ‘ ' i * > > ■ i ‘ ‘ 1 1 i ’ ■ ■ ' i 1 ' ■ • 3.80 4.00 4.20 4.40 0- ■ ■ i ■1 ■ ■ i1 1’’ i ‘■ i ■ TT ----- m/z 86.00 88.29% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #34671: Ethanamine, N-ethyI-N-[(ethylthio)methyl]- 86

5000 3.80 4.00 4.20 4.40 42 58 m/z 41.10 54.56% —lll+ map „MMMMoo 70 0-mm । ...... /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #34648: Propanal, 2-methyl-2-(methylsuIfinyl)-, oxime 41 85

3.80 4.00 4.20 4.40 5000 28 m/z 44.10 40.08%

miz-> 0- 10 15

— 20 30 k 1A8,57.e4.76, I 40 50 69

90 100 110 120 130 140 150 60 70 80 WAAMWMHt Abundance #34683: Dianhydromannitol ’—I 86 3.80 4.00 4.20 4.40

otu m/z 48.10 37.90% 5000 43 58 69

n/z-> 0 ■' i ■ ■' ■ i1 ■'' i ■ 10 20 30 +,51l4z,177 J IUuuntuemmmuHg 40 50 60 70 "i 80 , 96 103 114 131 146 90 1W 110 120 130 140 150 3.80 4.00' 4.20 4.40

12735.D 060302.M Mon Jun 10 11:22:47 2002 Page 9

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