GCMS analysis results for sample AE12162, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Ethane, fluoro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.79 1.05 ug/L 640428 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane, fluoro- 48 C2H5F 000353-36-6 9 2 Ethane, fluoro- 48 C2H5F 000353-36-6 7 3 1,4-Dioxin, 2,3-dihydro- 86 C4H602 000543-75-9 4 4 Ethenamine, N-methyl-N-nitroso- 86 C3H6N2O 004549-40-0 3 Abundance Scan 122 (3.796 min): 12162.D (-120) (-) m/z 86.00 100.00% 47 85

58 5000 51 38 43 3.40 3.60 3.80 4.00 4.20

niz-> 0- mmmmmmHmtmHmmH##HHH+p 4 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z 47.00 / 86.67% Abundance #12274: Ethane, fluoro- 47

5000 3.40 3.60 3.80 4.00 4.20 33 27 m/z 58.10 60.65%

miz-> 0- —++ —43l— 1519 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 TpTTTpTn-rpTTTpTTTp-TTTTT^^

Abundance #111001: Ethane, fluoro- 47 3.40 3.60 3.80 4.00 4.20 5000 m/z 51.10 46.18% 27 33 —/

niz-> 0- m —420++ 7.43L51.56 ’I’ 37 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 65 rrrrTTTp-rTTp-rrrpTrrp-^^

Abundance #701: 1,4-Dioxin, 2,3-dihydro- 30 3.40 3.60 3.80 4.00 4.20 86 m/z 49.10 35.12% 5000 58

26 0 ......................... —0 1 36 42 47 54 1. 71 7781 ._____ m/z-> 0 5 10 15 20253035404550556065 70 75 80 85 90 95 3.40 3.60 3.80 4.66 4.20

12162.D 052202.M Wed May 29 09:55:11 2002 Page 5

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