GCMS calibration table data, sample AE10517, May 22, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Ethane, fluoro- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

3.98 0.77 ug/L 479386 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethane, fluoro- 48 C2H5F 000353-36-6 19 2 Ethane, fluoro- 48 C2H5F 000353-36-6 9 3 l-Propanethiol 76 C3H8S 000107-03-/ 9 4 2-Butanone, 4-hydroxy -______________ 88 C4H802 1000197-37-3 3 Abundance Scan 154 (3.984 min): 10517.D (-152) (-) m/z 47.10 100.00%

5000 43 47 51

58 88 MAP... 35 84 3.60 3.80 4.00 4.20 4.40

niz-> 0- +4 ।....|,|.... t... H . + TITT ‘“I" 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 IImmO—BEEB0a"T TJTTTrfTT m/z 51.10 68.93% Abundance #111001: Ethane, fluoro- 47

5000 27 33 3.60 3.80 4.00 4.20 4.40 m/z 43.10 54.85%

n/z-> 0- —0 2.4.20.24 +4+ 37./4311,5511, 56 65 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Ay"TVW"AMN"M#e Abundance #12274: Ethane, fluoro-" 47 3.60 3.80 4.00 4.20 4.40 5000 m/z 88.00 51.94%

0- 1519 n)—mmmea—nmamBp —ment—, m— i. 27 a11 33

—3l— . j।p.. i p. i. t।j.... P. J’1***'- miz-> 0 5 10 15 20253035404550556065 70 75 80859095 Abundance #111007:1-Propanethiol 27 43 47 3.60 3.80 4.00 4.20 4.40 76 m/z 58.10 40.05% 5000 39

15 33 61

miz—> 0 "o" T „244l —ll I, 57 I 69 73 11}I:M 11IIIjllH | N 1111111 | Hip... p ...p 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 p. 3.60 3.80 4.00 4.20 440

10517.D 052202.M Wed May 22 11:48:09 2002 Page 7

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