GCMS calibration table data, sample AE10517, May 22, 2002

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Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013285–000013308

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 1-Buten-3-yne, 1-chloro-, (Z) - Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

4.03 1.66 ug/L 1038620 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l-Buten-3-yne, 1-chloro-, (Z)- 86 C4H3C1 020374-90-7 /0 2 Crotonic acid 86 C4H602 003724-65-0/9 3 l-Buten-3-yne, 1-chloro-, (Z)- 86 C4H3C1 020374-90-/ 7 4 1,2,3-Butatriene, 1-chloro- 86 C4H3C1 020658-21-/3 7 Abundance Scan 162 (4.031 min): 10517.D (-160) (-) m/z 51.10 100.00% 51 86

5000

43 29 37 5/40 82 3.60 3.80 4.00 4.20 4.40 ' miz-> ol 11’8 l 58 I " " I r'1 ‘ 1 “ ‘ * I H 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ‘I ' " I “ 1 ‘ I “ ' ‘ 1 ‘ ‘ ‘ ‘ m/z 86.00 83.06% Abundance #12406:1-Buten-3-yne, 1-chloro-, (Z)- 51 86

5000 । ■ ■ ■ • । ■ ■ ■ ■ । ■1 ‘ । ‘ ‘ । ■ 3.603.80 4.00 4.20 4.40 m/z 43.10 26.07%

niz-> 26 30 37 43 48 ■..... 6063 ..... 7174..... 83 Of TTWPIPPITTTTTTTTTTHT Tu)uUvmmgoptt 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 49 mm Abundance #116766: Crotonic acid 41 85

3.60 3.80 4.00 4.20 4.40 5000 m/z 48.05 19.73% 69 27 3& 45 15

5+1218,241 334 4—TIH 5053 5760 66 72 Of /z-> 10 15 20 2i5 30 35 40 45 50 55 60 65 70 75 80p85 90’95" Abundance #111070:1-Buten-3-yne, 1-chloro-, (Z)- I ' ‘ ' I ' ' ‘ ‘ I ‘ ‘ ‘ I ‘ ' 1 ' I ‘ ‘ ' 51 86 3.60 3.80 4.00 4.20 4.40 m/z 87.95 19.44% 5000

60 n/z-> 0 ., ।. .. . 1 . .. 11 11 11 |. , i. ।. .. , ।.. ■ q>vi 11 11 11 । ■ ( 11 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 mappampospat 89-7 3.60 3.80 4.00 4.20 4.40

10517.D 052202.M Wed May 22 11:48:11 2002 Page 8

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