GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060702\12739.D Vial: 15 Acq On 7 Jun 2002 7:58 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Ethanamine, N-ethyl-N-[(eth... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 3.94 1.65 ug/L 1318610 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanamine, N-ethyl-N-[(ethylthi... 147 C7H17NS 003492-79-3 9 2 1-Propanol, 2-(dimethylamino)-2-... 117 C6H15NO 007005-47-2 k 3 2-Butenoic acid, (E)- 86 C4H602 000107-93-7 7 4 Ethenamine, N-methyl-N-nitroso- 86 C3H6N20 004549-40-/6 5 Abundance Scan 147 (3.943 min): 12739.D (-145) (-) m/z 86.00 100.00% 86

5000 41 49 70 ■ ' i ...................... ... । . । > > j । । । । । ■ 35 3.60 3.80 4.00 4.20 0- 1 ' ! p=) । i i i > । i JI' i [') Ll, ' ' ■ l---- l - 01 •I411114*’’I m/z 41.10 30.17% miz-> 10 20 30 40' 50 60 70 80 90 100 110 Abundance #34671: Ethanamine, N-ethyl-N-[(ethylthio)methyl]- 86 WM*rWAso 5000 ‘ ' I ' ' ‘ ‘ I ‘ ' I ■ ‘ ‘ ‘ 1 ‘ ‘ 1 1 3.60 3.80 4.00 4.20 42 58 m/z 49.10 17.90% 47 , 70 75

niz-> 0- n-i-i-rr i । i > i ■ । i i i > [ l I l TT+ 10 20 30 40 50 60 70- 1——— r 111 1 80 i.................................. 1 I 1 1 1 1 i '•' * i 90 100 110 Abundance #34755:1-Propanol, 2-(dimethylamino)-2-methyl- 86 ■ ■ i ■1 ■ ■ i ■ ■ ■ ■ । • ■ ■ ■ । ■ ■ ■ ' ।1 3.60 3.80 4.00 4.20 m/z 48.05 12.96%

"AAwnko 5000

44 56 72 O■ ■ i ■ 15 ■ i ■ 31 32—T ——— 1--194— MMA n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #116768:2-Butenoic acid, (E)- • ■ i ■ ■ ■ • i ■ • ■ • i ■ • • • i ‘ ■ 1 r' 86 3.60 3.80 4.00 4.20 m/z 70.00 11.96% 41 5000 69 AAaW, ah 4 0 ...... 111139 11,50. ,57 62 475 miz—> 10 20 30 40 50 60 70 80 90 100 110 3.60 3.80 4.00 4.20

12739.D 060302.M Mon Jun 10 11:51:02 2002 Page 7

NYC-WTC_000015293