GCMS sample AE12761 results, June 10 2002

NYC 9/11 Public Portal Document ulorary searen compound Keport

Data File C:\MSDCHEM\l\DATA\060602\12762.D Vial: 8 Acq On 6 Jun 2002 5:00 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 12 2-Propanone, 1,1,1-trichloro- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 5.93 0.36 ug/L 258588 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 64 2 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2/9 3 Butane, 2,2,3,3-tetranitro- 238 C4H6N4O8 020919-97-5 9 4 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 Abundance Scan 486 (5.935 min): 12762.D (-480) (-) m/z 43.10 WO. 00% 43

5000

5.60 5.80 6.00 6.20 01 ■ ■ । • ■ ■ ■ ।1 ■1 ■ i1 37, --- 49 ■ n 63 82 97 I■ 119125 1 * * ' ' I * ‘ ‘ ‘ I ' ‘ * * I ' * ‘ ' I ‘ ' m/z 124.90 9.42% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877:2-Propanone, 1,1,1-trichloro- 43

5000 5.60 5.80 6.00 6.20 m/z 126.90 7.68% 15 27 36 76 83 91 9/ 110117 125 0! — '■''■•I "''''Tl 1.49.55.93 11 11 • ■ i ■ ■ ■ ''I 1 1 ■ ■ I • • '’''i' ■ • ■ i ■ • miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3861: 2-Propanone, 1,1-dichloro- 43 ■ ■ । ‘ ■ i ■ ■ 1 ■ । • i ■ ■ ■ ■ । 5.60 5.80 6.00 6.20 5000 m/z 47.00 6.40%

15 27 ol ■ ■ । > i I • • 11 It I i 36 , 49 55 63 76 83,93 125 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3995: Butane, 2,2,3,3-tetranitro- ■ ' I 1 ■ ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ' i ' ' ' ■ i 30 43 5.60 5.80 6.00 6.20 m/z 97.00 6.35% 5000 53 15

■n/z-> +374 0 , ■ ■ 11 ib-, । 10 velenjos 20 30 40 50 60 69 86 70 80 90 100 110 120 130 1 rl ■ ■1 ■ I ■ ■1i ' ■ ■1 i ■1 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■' ■ ' i ■ ' ■ ■ i ■ ■ 5.60 5.80 i ' ■ ■ • i ■ ■ ■ ■ i 6.00 6.20

12762.D 060302.M Mon Jun 10 10:26:47 2002 Page 15

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