GCMS sample AE12761 results, June 10 2002

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Data File C:\MSDCHEM\l\DATA\060602\12762.D Vial: 8 Acq On 6 Jun 2002 5:00 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 13 Acetyl chloride Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 5.97 0.44 ug/L 315155 1,4-dichlorob'enzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetyl chloride 78 C2H3C10 000075-36-5 2 2 1,3-Dioxane-2-propanol, 2-methyl- 160 C8H16O3 036651-31-72 3 2 -Nonanone, 9-hydroxy- 158 C9H18O2 025368-56-3 2 4 Ethyl Chloride 64 C2H5C1 000075-00-3 2 Abundance Scan 491 (5.964 min): 12762.D (-489) (-) m/ z 43.10 JOO.00% 35 43

5000

58 5.60 5.80 6.00 6.20 6.40 !’! 110L 86 101 | 01 ‘ 1+11‘1++‘‘IT +11 1111'I1PmTT i ■ ■ • * i * • • * r ■' ■ i *4 ■ ■ i * ‘ m/ z 35.10 85.01% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance 43 #3868: Acetyl chloride YMMANW/ A

15

"w 5000 11**’ i ‘ * 560 5.80 6.00 6.20 6.40 36 63 m/z 47.00 22.82% 28 01 —1 |'I r pl-l la I1- 1501 —***—— 78 miz-> 10 20 30 40। 50 60 70 80 90 100 110 120 130 140 150 Abundance #5776:1,3-Dioxane-2-propanol, 2-methyl- 43 58

5.60 5.80 6.00 6.20 6.40 5000 m/z 48.10 21.95%

Ot ■ ■ i' ■ ■ ■ i ■ ■' ■ i ‘11 ■ I 59,4 ................ 84

1, T1 1 1 ' 1 1 1 1 1 I ' 1 1 ' 101 145 i»* * *!•*•■i• ■ • * i ■ *'' i *'111 * • • ■ i * • "MWaaiyinA.. Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #5782:2-Nonanone, 9-hydroxy- 43 58 5.60 5.80 6.00 6.20 6.40 m/z 58.10 20.79%

5000

71 82 0 ‘ 1 ! । 1 1 1 1 1 1 ‘ ‘ 1 1 rr ll- 1 l r It Tur 97........... I•■>.।। ■1> * । * ■111111111 111 111111 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 5.60 5.80 6.00 6.20 6.40

12762.D 060302.M Mon Jun 10 10:26:50 2002 Page 16

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