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GCMS analysis results, sample AE12324, June 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry results for sample AE12324 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014303–000014329

Folder label: “GCMS X 5/24/02 A 5/29/02

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Scanned page image, NYC-WTC_000014319
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NYC 9/11 Public Portal Document Llbrary searcn compound Keport

Data File : C:\MSDCHEM\l\DATA\052902\12324.D vial: 12 Acq On : 29 May 2002 7:03 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Acetic acid, dichloro- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 4.18 1.33 ug/L 897797 1,4 -Dichlorob'enzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, dichloro- 128 C2H2C12O2 000079-43-6 17 2 Methylene Chloride 84 CH2C12 000075-09-2/9 3 Methylene Chloride 84 CH2C12 000075-09-2 9 4 Methylene Chloride 84 CH2C12 000075-09-2 9 Abundance Scan 187 (4.178 min): 12324.D (-185) (-) m/z 49.10 100.00% 49

84 5000 37 98

3.80 4.00 4.20 4.40 4.60 0 —Pmmmr ‘1 * * * ‘ 1 ‘ ‘ ’ ’ I * H m/z 48.00 60.38%

""MWuwps ■ ■ i ■ ■ ■ • i1 ■ ■ ■ i ■ ‘

iz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12316: Acetic acid, dichloro- 43 84

5000 3.80 4.00 4.20 4.40 4.60 29 m/z 84.00 53.46% A 13 I 41 = 65 76 miz-> OTT > 11 j lb i'i 11 0 -4 56 . । . 'T1 ■ "'i "" 111 i-i 11 .1 1 93 1 113 128 । j • ■ ■ ■ । । । ■ । । । । 1 1 । • ■ • 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #111041: Methylene Chloride 49 84 3.80 4.00 4.20 4.40 4.60 5000

_________ 29 41., |, niz-> 0- 111—211—9919—0214 0 +p*mm**mPPI 10 20 30 40 50 60 70 80 90 100 110 120 130 . 33.11 Abundance #12327: Methylene Chloride 49 3.80 4.00 4.20 4.40 4.60 84 m/z 98.00 44.62% 5000

14 24 35 42 h 0 I I I I- r r f| rill I ill || । ili ’t । JI ,I " ■ ■ l ■ “ ■70 l ■ “ 111 niz-> 0 10 20 30 40 50 60 70 80 SO * 100 110 120 ”1'36 3.80 4.00 4.20 4.40 4.60

12324.D 052202.M Mon Jun 03 10:52:10 2002 Page 12

NYC-WTC_000014319

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NYC-WTC_000014319Source: NYC Law Department, mirrored locally

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