GCMS analysis report sample AE09519, May 23, 2002

NYC 9/11 Public Portal Document Llorary searen compound keport

Data File : C:\MSDCHEM\1\DATA\052102\9519.D Vial: 14 Acq On : 21 May 2002 11:55 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 Ethyl Chloride Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 4.76 0.69 ug/L 411935 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 9 2 Borane, trifluoro- 68 BF3 007637-07-2/2 3 Boron trifluoride etherate 142 C4H10BF3O 000109-63-7 2 4 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 2 Abundance Scan 286 (4,760 min): 9519.D (-284) (-) m/z 49.10 100.00% 49

5000 84 38 4 40 4.60 4.80 5.00 5.20 58 0- ' i ■ ■ ■ ■ i ■ • ‘ ■ i ‘ Iur i ■ ■' 11 ■ • ■ • i ■ ■ ■ • i ■ I ... m/z 84.00 35.69% mfe-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #107943: Ethyl Chloride 23

64 50001 4.40 4.60 480 5.00 5.20 49 m/z 47.10 ", 33.17% 35 15 I 0- । ■ ■ ■ ।111 — 1144**14***1*1*414/44*1/1/:41144/1144 n/z—> 0 10 20 30 40 50 60 70 80 .90 100 110 120 130 Abundance #12321: Borane, trifluoro- 49

4.40 4.60 4.80 5.00 5.20 5000 m/ z 51.10 32.66% *

11 19 30 38 68 0-' ■ " I1' ■ ■ ''i'' 1' I " '' i ■' l'1 * ‘ t * • * 11.... j.... t. ।i.... i.... t,, miz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1099: Boron trifluoride etherate ■ ■ ■ i ■ ‘ ■ i ‘ ■ i ' ■ ■ ■ i ■ ■ ■ ' i 1 31 4 40 4.60 4.80 5.00 5.20 m/z 48.00 22.88? 59 5000 45 74

15 n/z-> 0- o • • । 10 ii - +29 1, 39,1,,/ ,, , HHT 66 . .81 93 127 20 30 40 50 60 70 80 90 100 110 120 130 Wp-rT-T-p-r-r-rT-rT-r-ry-r-r-rTy-r-^^ ■ ' i ' ■ ■ 1 i ■ ■ ■ • i 1 1 ‘ ■ i ■ 1 ‘ ' I ■ 4.40 4.60 4.80 5.00 5.20

9519.D 052202.M Wed May 22 11:32:38 2002 Page 9

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