GCMS reference standard results, June 10 2002

NYC 9/11 Public Portal Document Llbrary searen compound Report

Data File C:\MSDCHEM\1\DATA\060602\12743.D Vial: 6 Acq On 6 Jun 2002 3:22 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 Ethyl Chloride Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.99 1.36 ug/L 970159 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethyl Chloride 64 C2H5C1 000075-00-3 38 2 1,3-Diamino-2-propanol 90 C3H10N2O 000616-29-52 3 Methylene Chloride 84 CH2C12 000075-09/2 2 4 2 -Chloroethanol 80 C2H5C10 000107-07-3 2 Abundance Scan 155 (3.990 min): 12743.D (-153) (-) m/z 88.00 Z00.00% 49 88

5000 35 44 85 3.60 3.80 4.00 4.20 4.40 01 nyossigasgsasga..... 481, 1‘ 11 01111111/44 m/249.10 90.34% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride 23

64 5000 3.60 3.80 4.00 4.20 4.40 49 m/z 47.05 74.15% 25 35

mfe-> 0! —AH1215 T[T* 5 10 15 20 25 3031.,138. n,. 7 35 40 45 50 55 60 65 70 75 80 85 90 95 I1'*‘I**“I'1''I'*"I*’‘'I!"‘I

Abundance #830:1,3-Diamino-2-propanol 30 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 1 1 1 1 ' ■ i ■ ■ 3.60 3.80 4.00 4.20 4.40 m/z 35.10 45.32%

MMMo. 5000 60 18 42 71 35 15 H ’wy Ar mfa-> 0 111।.111111 Iai. ’ l’+4’1’’’41+**’1** 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111040: Methylene Chloride 49 3.60 3.80 4.00 4.20 4.40 84 m/z 44.00 37.74% 5000

35 14 88 0 THH 11111 252811132 ,38441 70 . i .11 in i|HHrr 152 + I’ ‘ i ■ ■ ■ ■ i" ■ ■ i ■ “ ■ 11 ■ ■ ■ i ■ • • • i • ■1 n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20 4.40

12743.D 060302.M Mon Jun 10 10:21:55 2002 Page 12

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