GCMS analysis report sample AE09682, May 23, 2002

NYC 9/11 Public Portal Document ubrary searen compound Keport Data File : C:\MSDCHEM\1\DATA\052102\9682.D Vial: 18 Acq On : 22 May 2002 3:11 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 4 Ethyl Chloride Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

3.83 1.32 ug/L 930160 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 4/ 2 Borane, trifluoro- 68 BF3 007637-07-2 2 3 2-Chloroethanol 80 C2H5C10 000107-07-3/2 4 Boron trifluoride etherate 142 C4H10BF3O 000109-63-/ 2 Abundance

5000 Scan 128 (3.831 min): 9682.D (-126) (-)

43 49 442 m/z 49.10 100.00%

36

RKzkpGBsnSswJSasss 85 3.40 3.60 3.80 4.00 4.20 ob ■ i ■ “ ■ i • ■" r ■ ■' I “ “ i' ■ “ i “ ’IF THTTT mmmmpmm miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 K 70 75 80 85 30 Abundance #107943: Ethyl Chloride

64 5000 3,40 3.60 3.80 4.00 4.20 49 m/z 48.10 20.82% 25

n/z-> Abundance Ob 0 1215 TyT —4 31.4728,144417..SQ, TBuu—n— 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 67 BB—p—BBgnn #12321: Borane, trifluoro- 40 ouy""hpo i ■ ■ ■ ■ । ■ ■ ' ■ i‘ ■ • • i ■ ■ ■ • i ■ ■ •

3.40 3.60 3.80 4.00 4.20 5000 m/z 41.05 18.56%

11 19 30 38 68 0b 11 > th pass TPTTTL i > 111111 > 11111. i ■ । ■ i TmTTmTPTT m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #108328:2-Chloroethanol 31 3.40 3.60 3.80 4.00 4.20 m/z 50.10 16.29%

5000 27 44

40,53 576063 ob «• ’ I ‘ ‘ ‘ ’I “ 11 I ‘ " '! " ‘ ’ I ‘ T .353841 ,Hhhmmmmp 76 8° n/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 3.40 3.60 3.80 4.00 4.20

9682.D 052202.M Wed May 22 11:46:45 2002 Page 6

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