GCMS analysis results, sample AE12321, June 2002

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Data File : C:\MSDCHEM\l\DATA\052902\12321.D Vial: 9 Acq On : 29 May 2002 4:36 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Ethyl Chloride Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

4.01 1.65 ug/L 1129240 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Ethyl Chloride 64 C2H5C1 000075-00-3 8 2 Borane, trifluoro- 68 BF3 007637-07-2/2 3 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 4 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17/0 2 Abundance Scan 158 (4.007 min): 12321 .D (-155) (-) m/z. 49.10 100.00% 49 86

5000

37 42 3.60 3.80 4.00 4.20 4.40 Of 1 ■ i ■ • ■11" “ i ■" ■ i “ “ i • i‘ "’IT m/z 86.00 73.09% mlz—> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride 28

64 5000 3.60 3.80 4.00 4.20 4.40 25 49 m/z 51.10 27.00% _/ of mp rr 1215 ............ 1,1......^! 67 miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12321: Borane, trifluoro- 49 3.60 3.80 4.00 4.20 4.40 5000 m/z 48.05 21.84%

Of 11 19 30 11111111111 1 !'| 111111 n 1111111111111 > 11 (11 38 68 111., 1111111 < । > j > > I > । > > 111 < 1 > 11 i ■ । > 1111111 ■ 11 ■ „/"Mmpaw niz-> 0i 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108328:2-Chloroethanol 31 3.60 3.80 4.00 4.20 4.40 m/z 37.10 15.48% 5000 27 44 49 of■ “' i1' ■ ■ i1 • ■ ■ i ■ ■ ■' i ■ ■ ■ ■ 353841 ....................................... | 53 576063 HHhmthmmmmmmpm 76 80 i■ T 1111 iin 111 /z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20 4.40

12321.D 052202.M Mon Jun 03 10:48:28 2002 Page 10

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