GCMS analysis results, sample AE12321, June 2002

NYC 9/11 Public Portal Document Llprary searen compound Keport

Data File : C:\MSDCHEM\l\DATA\052902\12321.D Vial: 9 Acq On : 29 May 2002 4:36 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integfator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Dicyandiamide Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

3.95 1.03 ug/L 700810 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dicyandiamide 84 C2H4N4 000461-58-5 7 2 Krypton 84 Kr 007439-90/9 4 3 2-Butenal, 3-methyl- 84 C5H80 000107-86-8 4 4 Thiophene 84 C4H4S 000110-02-1 4 Abundance Scan 148 (3.949 min): 12321.D (-146) (-) m/z 84.00 /100.00% 47 84 88 35 5000 44 ’1’1’*I**I’*’1’**’I* 58 3.60 3.80 4.00 4.20 0- - m/z 47.00 93.97%

MMMo 1118 ’38 ’414 11 ■1 ■ ■ i ■ ■ niz-> 30 35 40 45 50 556065 70 75 80859095 Abundance #116556: Dicyandiamide 43 84

5000 68 ■ ■ i ■ ■ ■ ■ i ‘ ' ■ i ■ ' 1 1 i ' 1 ' ' I ' 3.60 3.80 4.00 4.20 m/z 88.00 79.58%

miz-> 01

Abundance 0 ■11.... 30 < • •. । 53 35 56 • i ■ 11 40 ■ । ....... 45 > 11 * * ■ i ■ 111 11—’ 50 55 60 65 70 #33829: Krypton 75 80 111111'111 P 1 85 90 95

84 "Peanaw ' 1 I ' 1 1 ■ i ■ ■ ■ ■ i 1 r 1 1 1 1 1 1 1 I ' 3.60 3.80 4.00 4.20 50001 m/ z 35.10 61.48%

42 MW “ WMWA N,Mpd 0- -n-p-r-n-p- lhgoookgooni r11111111111111111111 <11180 111 -r-r-p-r-r-rp-T miz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116598:2-Butenal, 3-methyl- 84 3.60 3.80 4.00 4.20 m/z 86.90 36.19% 5000 41 55 . A1 50 . 65 69 0 HTT -H— 1' " I " ■' I " ■111 ■ ■' i “ ' ■ i ■' ’ I''1' I ‘'1 'I " TT n/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

12321.D 052202.M Mon Jun 03 10:48:28 2002 Page 9

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