GCMS Method 508 sample analysis results, April 9 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020409\6337.D Vial: 6 Acq On 9 Apr 2002 7:49 pm Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1...\SCANAPR0902. M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Ethyl Chloride Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.29 0.28 ug/1 182794 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 4 2 2-Butyne-1,4-diol 86 C4H6O2 000110-65-6 3 3 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 2 4 Ethanol, 2,2-dichloro- 114 C2H4C12O 000598-38-9 2 Abundance Scan 36 (3.291 min): 6337.D (-21) (-) m/z 49705 100.00% 4^ 8000 84 6000 43 74- 4000 71 1" ’ ■ I " " I ’ I ■'' .... I.... I.... I f. . I... 11..... I.... I.... J .. T .'' I " '. I ■ 3.20 3.30 3.40 3.50 3.60 3.70 m/z 84.00 70775% ■n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride

64 5000 3 20 3.30 3 40 3.50 3.60 3 70 49 "m/z 86700 66.60% 35 I I

5 . ul.. .... 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108388: 2-Butyne-1,4-diol 29 39 57

3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 47710 55.12% 68 2< 51 43

■nA-> 5 ...... lllllllsj Jtajhe 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34862: Imidazol, 4-fluoro- 85 _a20 3J03;4g^,50JW_370_ m/z 74717 43.69% 5000

59

Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.30 3.40 3.50 3.60 3.70

6337.D SCANAPR0902.M Thu May 02 14:04:58 2002 Page 3

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