GCMS analysis report sample AE09519, May 23, 2002

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Data File : C:\MSDCHEM\1\DATA\052102\9519.D Vial: 14 Acq On : 21 May 2002 11:55 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 2-p-Nitrobenzoyl-l,3,5-trib... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

5.18 0.24 ug/L 141350 1,4 -Dichlorob'enzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual l 2-p-Nitrobenzoyl-l,3,5-tribenzyl... 569 C33H31NO8 1000129-85-6 2 2 4-Chlorobuten-3-yne 86 C4H3C1 040589-38-6 2 3 Nitrosyl chloride 65 CINO 002696-92/6 2 4 Ethyl Chloride 64 C2H5C1 000075-00-3 1 Abundance Scan 357 (5.177 min): 9519.D (-353) (-) m/z 35.10 100.00% 35 51

5000 43 84 88 TI r [**‘I 47 480 5.00 5.20 5.40 5.60 0 ‘ “ I" - m/z 51.10 72.27%

MML. • ■ । • •.. । ‘ i “1 ■ i • * * * t ‘1 *1 r *' * H * ■ ‘ I “ “ I “ 1 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12372:2-p-Nitrobenzoyl-l ,3,5-tribenzyl-.alpha.-d-ribose 51

5000 4.80 5.00 5.20 5.40 5.60 41 45 m/z 84.00 34.58%

niz-> of ---4 i5 10 15 20253035404550556065 70 75 808590 95 558@274*. Abundance #12405:4-Chlorobuten-3-yne 5ft 86

4.80 5.00 5.20 5.40 5.60 5000 m/z 88.00 33.73%

mfz~> 0 i" " i" ■ ■ i ■ • ■' i ■ ■" i ■" ■ i ■" ■ i • i" " i “ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 60 '‘i"1 MMP"yMwp/Aop., Abundance #713: Nitrosyl chloride 3) 4.80 5.00 5.20 5.40 5.60 m/z 43.10 21.63% 5000 35 14 I 4649 0 ।....।... 111... ।... 11.. T+TTp-rrrrrTT+TTTTTp-rrTp-rTTp-rTTyrrrrp-rr^^ m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.80 5.00 5.20 5.40 5.60

9519.D 052202.M Wed May 22 11:32:40 2002 Page 10

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