GCMS analysis results, sample AE12476, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12476.D Vial: 18 Acq On : 29 May 2002 11:56 pm Operator: McLean . Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ** ******************************************************************* Peak Number 6 2-Chloroethanol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.93 0.66 ug/L 487960 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 2 2-p-Nitrobenzoyl-l,3,5-tribenzyl... 569 C33H31NO8 1000129-85-6/2 3 Ethyl Chloride 64 C2H5C1 000075-00-3 2 4 2-Chloroethanol 80 C2H5C10 000107-0X3 2 Abundance Scan 145 (3.931 min): 12476.D (-144) (-) m/z 49.10 100.00% 49

5000

58 70 ' ■ ‘ I ‘ ‘ ‘ ‘ I ' ‘ ‘ ' I ■ ‘ ' 1 ' ' ' ' I 38 . ll I | 1421 I > | l 83 87 3.60 3.80 4.00 4.20 0! (1.... 1 ... I | I 1 I I | ■ 1 ri | 1 11 u ‘ i ■ “ ■ i *' ■ ■ mTTTTT m/z 51.10 61.77% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 _/ Abundance #108328:2-Chloroethanol 31

5000 1 ■ i ■ ■ ■ ■ i ‘ 1 ■ ■ i ■ ■ • ■ i ■ ■ ■ • ।

44 3.60 3.80 4.00 4.20 27 m/z 47.10 23.96% 49 353841 ,53 576063 76 80 01 T —Hmmmp nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12372:2-p-Nitrobenzoyl-1,3 5-tribenzyl-alpha.-d-ribose 51 ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i ■ ‘ ■ i ■ ■ ■ ■ i 3.60 3.80 4.00 4.20 5000 m/z 70.10 18.96%

0! ’T 41 45 ...... 5558 6265.69 11111111 111 1111111 TOmiT l1 ‘ ” I miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride TII TI ’dI 3.60 3.80 4.00 4.20 m/z 58.00 15.94% 64 5000-

49 25 35 1215 0 ’’I “ TMH im 31 Hr +38----Al-I4 67 60 111"9"1011’5702101322111777TT *I "tt 4 11 1 n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 | 3.60 3.80 4.00 4.20

12476.D 052202.M Mon Jun 03 11:33:58 2002 Page 9

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