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← Document results/DEP Box 15/GCMS X 5/31/02 A 6/3/02
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GCMS analysis results for sample AE12224, June 2002

Machine-extracted title · confidence 100%

Laboratory report listing concentrations of volatile organic compounds including nitrosamines and chlorobenzenes in sample AE12224.

NYC-WTC_000015063–000015074

Folder label: “GCMS X 5/31/02 A 6/3/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\JUN0302\12224.D Vial: 6 Acq On 3 Jun 2002 2:05 pm Operator: Sample re-ext Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) , Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 8.07 0.83 ug/1 60275 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 3 -Hexanol, 4-methyl- 116 C7H160 000615-29-2 28 3 5-Hexen-2-one 98 C6H10O 000109-49-9 9 4 3-Hydroxy-2-pentanone____________ 102 C5H10O2 003142-66-3 9 Abundance- Scan 330 (8.072 min): 12224.D (-) m/z 43.00 100.00% 40

59 5000

101 1111 I' 7.80 8.00 8.20 8.40

miz—> m+ TTmag 83 49 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 , m/z 59.0.0 51.34% Abundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 1 ■ ‘ ■ i ■ 1 ' • i ‘ ■ i • ■ ■ ■ i ‘ ■ 7.80 8.00 8.20 8.40 m/z 58.00 18.99% 101 ,31 73 ।.. 11 > i ■. 11 > ।. 111.. ।. I.. 11.11111.. 111 11.11.111 ■ 111! ■ 11,,, ।, 11, ।, rn f i, r 83 101 11111,11,11,11111111111 ly, i,, ।, m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #3362:3-Hexanol, 4-methyl-

5000 41 50 ■ ' i ■ ■ 7.80 m/z 101.05 h. 8.00 8.20 8.40 16.83% 31 69 87 _____________________ 6 | , | 98 ‘ ‘*I‘*‘*I‘I*///I//*AAA/**-d***S*S****** m/z—> 5 10 15 20253035404550 55 6065 70 75 80859095 100105 Abundance #63205:5-Hexen-2-one ■ ■ i ■ ■ 43 7.80 8.00 8.20 8.40 m/z 41.00 9.06% 5000

27 55 15

m/z-> ................... 1’ u’1901—m30531—|0—9—00—38,.. —5030159—50.______________ 83 —0Tu_uTDpnp 98 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 MMAAAAA 7.80 8.00 8.20 8.40

12224.D GCMS0531.M Tue Jun 04 09:03:20 2002 Page 1

NYC-WTC_000015070

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NYC-WTC_000015070Source: NYC Law Department, mirrored locally

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