Laboratory report listing concentrations of volatile organic compounds including nitrosamines and chlorobenzenes in sample AE12224.
NYC-WTC_000015063–000015074Folder label: “GCMS X 5/31/02 A 6/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO 302\12224.D Vial: 6 Acq On 3 Jun 2002 2:05 pm Operator: Sample re-ext Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Bicyclo[2.2.1]hept-5-ene-2,3-d Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 38.54 0.78 ug/1 41519 Perylene-dl2 37.66 Hit# Of 5 Tentative ID MW MolForm CAS# Qual l Bicyclo^.2.1]hept-5-ene-2,3-dicarb 326 C15H2604Si2 056151-04-3 9 2 3-Iso opoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 9 3 Tris. rimethylsilyl)borate 278 C9H27BO3S13 004325-85-3 9 4 Hexahydropyridine, 4-[4 r 5-dimethoxy 221 C13H19NO2 000000-00-0 7 Abundance Scan 3649 (38.541 min): 12224.D (-) m/z 73.00 100.00% 73
5000 147 221 281 355 ■ i • ‘ ■ i 193 . 253 | ( 3271 429 38.20 38.40 38.60 38.80 96 I — 1 • i ■ ■ • -17r/111/*/1/11////*=11/1/-/-T/1/1//tIEoT m/z 147.10 48.87% miz-> 50 100 150 200 250 300 350 4TO 450 500 550 Abundance #46279: Bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylicacid, bis 73
5000 MAAAAA 38.20 38.40 38.60 38.80 .. 119 147171 209 245 m/z 221.10 46.54% ___ L 326 ■ ' i ' ■ ■ ■ i ■ ' ■ ■ i ‘ ■ i ■ ■ ■ ■ i ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ iz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 ■ ' i ■ ■ • ■ i 38.20 38.40 38.60 38.80 5000 m/z 207.00 26.95% 147 pMWWWAAkopaoAoo 221 281 ™ 4= ...... |....... I......... ................. ,561 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #39028: Tris(trimethylsily!)borate T M * I 73 221 38.20 38.40 38.60 38.80 m/z 281.00 / 24.22% 5000 263 133
miz—> 50 —4 100 150 ■ ■ i • ■ 1 ■ i ■ 1 ■ ■ i 1 1 1 1 i 1 1 1 1 i 1 r 1 '"r1 1 300 350 400 450 500 550 38.20 38.40 38.60 38.80 ‘
12224.D GCMS0531.M Tue Jun 04 09:03:20 2002 Page 2
NYC-WTC_000015071
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NYC-WTC_000015075
Laboratory report documenting GCMS analysis of sample AE12224 with surrogate recovery data and identification of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014690
Laboratory report documenting GCMS analysis of sample AE12571 conducted on June 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014670
Laboratory report documenting GCMS analysis of sample AE12539 conducted on June 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015093
Laboratory report documenting GCMS analysis of sample AE12285 with surrogate recovery data and identification of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015121
Laboratory report documenting GCMS analysis of sample AE12679 with surrogate recovery data and identification of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046340
Laboratory report documenting GCMS analysis of sample AE09334 conducted on May 8, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043667
Summary of GC/MS analytical results for sample AE08838 processed on May 7, 2002, including surrogate recovery data.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046321
Laboratory report documenting GCMS analysis of sample AE09587 conducted on May 17, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048737
GCMS laboratory report for sample AE05852 analyzed on April 23, 2002, by analyst DLV.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045516
Laboratory report documenting GCMS analysis of sample AE09451 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045462
Laboratory report documenting GCMS analysis of sample AE09447 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043686
Summary of GC/MS analytical results for sample AE08837 processed on May 7, 2002, including surrogate recovery data.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000015036
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12677 conducted on June 6, 2002.
Filed in the same folder
NYC-WTC_000015037
Administrative log sheet recording sample processing details and metadata for environmental testing conducted between May 31 and June 3, 2002.
Filed in the same folder
NYC-WTC_000015040
Laboratory report documenting a method blank analysis for GCMS testing of sample AE12224 to verify absence of contamination on June 3, 2002.
Filed in the same folder
NYC-WTC_000015054
Laboratory report documenting a method blank analysis for GCMS testing of sample AE12224 to verify absence of contamination on June 3, 2002.
Filed in the same folder
NYC-WTC_000015058
Reference gas chromatography-mass spectrometry analysis for sample AE12224, comparing results across multiple organic compounds with detection limits and reference values.
Filed in the same folder