NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\ JUNO 302\12224.D Vial: 6
Acq On 3 Jun 2002 2:05 pm Operator:
Sample re-ext Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 3 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
40.24 1.00 ug/1 53285 Perylene-d12 37.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4/5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 38
2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28
3 Pentanoic acid, 2-[(trimethylsilyl) 262 CllH2603Si2 055887-46-2 12
4 Butanoic J cid, 3-methyl-3-[(trimeth 262 C11H26O3S12 055124-90-8 12
Abundance Scan 3834 (40,240 min): 12224.D (-) m/z 73.0.0 100.00%
73
147
221
5000
355
281
T T
429
m/z-?
45
1
■ • i '
50
01/"
100
,
150
191
200 250
m
253
300 350
——
400 450 500 550
40.00 40.20 40.40 40.60
m/z 147.00 78.42%
Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7-
147 221
73
5000 AY) M40.00
MA. • : WWyA
40.20 40.40 ‘40,60
191 m/z 221.10 67.09%
279
L, "...
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
40.00 40.20 40.40 40.60
5000 m/z 207.00 34.99%
147
MoAoMMWhwooo
221 281
mz-> 50
' * i ‘
100 150 200
—
250
H300 327,350 415
1/4/ I1! 1111111". ' I ' ‘
400 450 500
519 561
550
Abundance #36156: Pentanoic acid, 2-I(trimethylsilyl)oxy]-, trimethyl
73 40.00 40.20 40.40 40.60
131
m/z 355.00 33.85%
5000
46 . 247
1’ ■ 1 ■ •
I li 2 |
‘ I**
mtt~> 50 1100 150 200 250 300 350 400 450 500 550
■ ■ 1 ■ ■
40.00 40.20 40.40 40.60
12224.D GCMS0531.M Tue Jun 04 09:03:21 2002 Page 3
NYC-WTC_000015072
OCR can misread numbers and units. Confirm readings against the page image before using them.