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GCMS analysis results for sample AE12224, June 2002

Machine-extracted title · confidence 100%

Laboratory report listing concentrations of volatile organic compounds including nitrosamines and chlorobenzenes in sample AE12224.

NYC-WTC_000015063–000015074

Folder label: “GCMS X 5/31/02 A 6/3/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\ JUNO 302\12224.D Vial: 6 Acq On 3 Jun 2002 2:05 pm Operator: Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

40.24 1.00 ug/1 53285 Perylene-d12 37.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4/5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 38 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 3 Pentanoic acid, 2-[(trimethylsilyl) 262 CllH2603Si2 055887-46-2 12 4 Butanoic J cid, 3-methyl-3-[(trimeth 262 C11H26O3S12 055124-90-8 12 Abundance Scan 3834 (40,240 min): 12224.D (-) m/z 73.0.0 100.00% 73 147 221 5000 355 281 T T 429

m/z-? 45 1 ■ • i ' 50 01/" 100 , 150 191 200 250 m 253 300 350 —— 400 450 500 550 40.00 40.20 40.40 40.60 m/z 147.00 78.42% Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221

73 5000 AY) M40.00 MA. • : WWyA 40.20 40.40 ‘40,60 191 m/z 221.10 67.09% 279 L, "... miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

40.00 40.20 40.40 40.60 5000 m/z 207.00 34.99% 147 MoAoMMWhwooo 221 281

mz-> 50 ' * i ‘ 100 150 200 — 250 H300 327,350 415 1/4/ I1! 1111111". ' I ' ‘ 400 450 500 519 561 550 Abundance #36156: Pentanoic acid, 2-I(trimethylsilyl)oxy]-, trimethyl 73 40.00 40.20 40.40 40.60 131 m/z 355.00 33.85% 5000

46 . 247 1’ ■ 1 ■ • I li 2 | ‘ I** mtt~> 50 1100 150 200 250 300 350 400 450 500 550 ■ ■ 1 ■ ■

40.00 40.20 40.40 40.60

12224.D GCMS0531.M Tue Jun 04 09:03:21 2002 Page 3

NYC-WTC_000015072

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NYC-WTC_000015072Source: NYC Law Department, mirrored locally

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