GCMS analysis results for sample AE12224, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO 302\12224.D vial: 6 Acq On 3 Jun 2002 2:05 pm Operator: Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3, 6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

42.35 1.07 ug/1 56962 Perylene-d12 37.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2y4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 32 2 2,6-Dimethyl-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 12 3 1,3-Benzodioxole, 5-[3-acetaminopro 221 C12H15NO3 000000-00-0 10 4 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 10 Abundance Scan 4064 (42.351 min): 12224.D (-) 73 147 221 5000 281 355

m/z-> 49 HH h 193 , vyaokyoohpdn 4234 40 60 80 100120140160180200220240260280300320340360380400420 r I 327 429 ■ । • ■ ■ ■ । ■ ■ ■ ■ । ■ ■" । 42.00 42.20 42.40 42.60 m/z 147.00 65.42% Abundance #41682:3,6-Dfoxa-2,4,5,7-tetrasilaoctane, 2,2,4,4.5,57,7- 147 2!1

73 5000 1 I1 t i ' i-p-n » | t I i t | r 42.00 42.20 42.40 42.60 191 m/z 221.10 60.10%

m/z-> —lll 279 -rq-rrrrpT11!h rep .11 j. 111 p . । .J. > > 11 > >. <,. > 111.11. [. CTTI’ < ’ 111111:1111 40 60 80 100120140160180200220240260280300320340360380400420 . ........... / ,

Abundance #44359:2,6-Dimethyl-3,4-bis(trimethylsilyloxymethyl)pyridi 73 221 r~T’ 42.00 42.20 42.40 42.60 5000 147 m/z 281.00 33.89%

■n/z-> Abundance 45 1, I '«J “ I > 1 “ “ I *1' ’ I * I - 178 4. 40 60 80 100120140160180200220240260280300320340360380400420 #27829:1,3-Benzodioxole, 5-[3-acetaminopropyl]- 221 2 > ■ 1111 > 111 ■ > 1111111 > । > । । ■ 111 < < 11 > ■ 1111111 j ■. 11 j 111 >! A42.00 42.20 42.40 42.60 m/z 355.00 27.62% 73 135 162 5000

104 49 ........... 1...... It....1?2. ________ . < ।।. 11. । < 11111 j 1. 1111, V. j । T11, < f 111111 rj 1111 TTTTTTr i1■1111 > i1ii1 ■ ] 111111ni11 m 11ii111 11 i I.1.1i I m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 42.00 42.20 42.40 42.60

12224.D GCMS0531.M Tue Jun 04 09:03:22 2002 Page 4

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