GCMS analysis results for sample AE12285, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report . L* Data File C:\HPCHEM\l\DATA\JUN0302\12285.D Vial: 8 Acq On 3 Jun 2002 4:04 pm Operator: Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.08 0.71 ug/1 51577 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 74 2 Acetones 58 C3H60 000067-64-1 9 3 5-Hexen-2 -one 98 C6H10O 000109-49-9 9 4 2-Hexanol, 2-methyl- 116 C7H160 000625-23-0 9 Abundance Scan 330 (8.077 min): 12285.D (-) m/z 42.90 100.00% 43

5000 59

101 7.80 8.00 8.20 8.40 51 83 mmmmmmmmmRHmmHmm m/z 59.00 50.91% miz—> 5 10 15 202530 35 404550556065 70 75 80859095 100105 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 —**9n—TTM-*1TT 59 7.80 8.00 8.20 8.40 m/z 58.00 19.87% 27 101 ......... |......... Il 49 83 83 । .... p... p ... p... p I ■. 11... p,. .p 11 Ip,. q-n n [ 1111 [, 11 > p i, i p rr, p ,, , p 111 p , i, p r, i p , 1, 111 > i p ,,, p m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62322: Acetone 43 ‘ ‘ I ‘ ‘ ‘ I ‘ ‘ ‘ ' I 1 1 1 1 1 1 1 1 1 7.80 8.00 8.20 8.40 5000 m/z 101.05 15.25% 58 27

m/z—> mmmmmmmmmHtmmmmmmmmmmmmmmmmm 5 10 15 20 25 3035404550556065 70 75 80859095 100105 Abundance #63205:5-Hexen-2-one 43 m/ Z • * । * 7.80 8.00 40.90 _y 8.20 8.40 5.78% 5000

27 55 15 — '... | |.1,.1 38,. 50. ____________.p,l83.p 98 * * i • * ■ ■ । * * i ■ • ■ ■ i ‘ ' <nfz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.80 8.00 8.20 8.40

12285.D GCMS0531.M Tue Jun 04 09:03:42 2002 Page 1

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