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GCMS reference analysis for sample AE12224, June 2002

Machine-extracted title · confidence 100%

Reference gas chromatography-mass spectrometry analysis for sample AE12224, comparing results across multiple organic compounds with detection limits and reference values.

NYC-WTC_000015058–000015062

Folder label: “GCMS X 5/31/02 A 6/3/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\JUN03 02\REF1.D Vial: 4 Acq On 3 Jun 2002 11:39 am Operator: Morgan Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 14:21 2002 Quant Results File:GCMS0531 .RES e- Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.62 178 669554 14.87 ug/1 99 36) Di-n-butylphthalate 27.41 149 867095 15.68 ug/1 100 37) Fluoranthene 29.11 202 698277 15.23 ug/1 98 3 9) Pyrene 29.78 202 719529 17.70 ug/1 98 40) Butylbenzylphthalate 31.93 149 308911 14.85 ug/1 99 41) Benzo(a)anthracene 33.42 228 451266 15.13 ug/1 99 42) Bis (2-e.thylhexyl) phthalate 33.71 149 393061 14.38 ug/1 100 43) Chrysene 33.55 228 458008 15.49 ug/1 99 45) Di-n-Octylphthalate 35.45 149 487983 12.27 ug/1 99 46) Benzo(b)fluoranthene 36.51 252 347746 15.07 ug/1 98 47) Benzo(k)fluoranthene 36.58 252 364598 15.24 ug/1 98 48) Benzo(a)pyrene 37.47 252 273161 12.26 ug/1 97 4 9) Indeno(1,2,3 -cd)pyrene 41.62 276 268970 12.88 ug/1 99 50) Dibenz(a,h)anthracene 41.69 278 227462 13.84 ug/1 98 51) Benzo(g,h,i)perylene 42.80 276 239417 14.06 ug/1 98

(#) = qualifier out of range (m) = manual integration REF1.D GCMS0531.M Mon Jun 03 14:30:34 2002 Page 2

NYC-WTC_0000 15061

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NYC-WTC_000015061Source: NYC Law Department, mirrored locally

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