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GCMS calibration results for VOCs, sample AE12535, June 2002

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Laboratory report showing GCMS calibration data for volatile organic compounds in sample AE12535 on June 3-4, 2002.

NYC-WTC_000014620–000014623

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\JUN0302\CAL10.D Vial: 2 Acq On 3 Jun 2002 9:41 am Operator: Morgan Sample Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 11:43 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.62 178 380245 9.27 ug/1 100 36) Di-n-butylphthalate 27.41 149 446977 8.87 ug/1 100 3 7) Fluoranthene 29.11 202 379065 9.08 ug/1 100 39) Pyrene 29.79 202 359334 9.10 ug/1 95 40) Butylbenzylphthalate 31.93 149 156111 7.73 ug/1 97 41) Benzo(a)anthracene 33.42 228 245037 8.46 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.71 149 210603 7.93 ug/1 98 43) Chrysene 33.55 228 259075 9.02 ug/1 99 45) Di-n-Octylphthalate 35.45 149 272561 6.81 ug/1 99 46) Benzo(b)fluoranthene 36.51 252 187732 8.08 ug/1 99 47) Benzo(k)fluoranthene 36.57 252 219637 9.12 ug/1 98 4 8) Benzo(a)pyrene 37.46 252 180898 8.06 ug/1 99 4 9) Indeno(1,2,3-cd)pyrene 41.62 276 160390 7.63 ug/1 99 5 0) Dibenz(a,h)anthracene 41.69 278 124873 7.55 ug/1 99 51) Benzo(g,h,i)perylene 42.80 276 135631 7.91 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS0531.M Tue Jun 04 11:34:27 2002 Page 2

NYC-WTC_000014622

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NYC-WTC_000014622Source: NYC Law Department, mirrored locally

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