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GCMS calibration data sample AE12094, June 2002

Machine-extracted title · confidence 95%

Calibration results for GCMS analysis of volatile organic compounds conducted on May 31, 2002.

NYC-WTC_000014964–000014967

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C: \HPCHEM\ 1 \DATA\MAY3102 \CAL4 0 . D Vial: 2 Acq On 31 May 2002 12:55 pm Operator: Morgan Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 9:20 2002 Quant Results File :GCMS0531. RES *e- Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.63 178 1683167 46.09 ug/1 100 36) Di-n-butylphthalate 27.41 149 2073875 46.24 ug/1 99 3 7) Fluoranthene 29.12 202 1725872 46.40 ug/1 98 39) Pyrene 29.79 202 1619165 43.82 ug/1 98 40) Butylbenzylphthalate 31.93 149 833880 44.12 ug/1 98 41) Benzo(a)anthracene 33.42 228 1227036 45.27 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.71 149 1127585 45.39 ug/1 99 43) Chrysene 33.55 228 1223838 45.54 ug/1 99 45) Di-n-Octylphthalate 35.45 149 1750886 44.48 ug/1 # 98 46) Benzo(b)fluoranthene 36.52 252 1088041 47.64 ug/1 99 47) Benzo(k)fluoranthene 36.58 252 1132632 47.84 ug/1 98 48) Benzo(a)pyrene 37.47 252 985464 44.66 ug/1 99 49) Indeno(l,2,3-cd)pyrene 41.63 276 932854 45.12 ug/1 99 50) Dibenz(a,h)anthracene 41.71 278 739428 45.44 ug/1 100 51) Benzo(g,h,i)perylene 42.83 276 757102 44.90 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0531.M Mon Jun 03 11:24:35 2002 Page 2

NYC-WTC_0000 14966

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NYC-WTC_000014966Source: NYC Law Department, mirrored locally

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