GCMS calibration data AE11284, DEP Labs, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3002\12095.D Vial: 14 Acq On : 31 May 2002 2:51 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Pentacosane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.11 0.72 ug/1 55467 1,4-Dichlorobenzene-d4 12.06 Hit# of Tentative ID MW MolForm CAS# Qual 1 Pentacosane 352 C25H52 000629-99-2 9 2 1 -Hexacosano 1 382 C26H540 000506-52-5 9 3 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 9 4 1-E/cosanol 298 C20H42O 000629-96-9 9 Abundance . Scan 334 (8.108 min): 12095.D (-) m/z 42.90 100.00% 43

5000

125

THr + 11................................. 61 83 . 7.80 8.00 8.20 8.40 1’11’0513112"’11E70EE"IT’’1’11’1711127E3UIOCCTT"""T"T m/z 124.85 15.51% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73718: Pentacosane 43

71 5000 • * » | 1 ‘ ‘ ‘ 1 1 ‘ TEt’ i । : i i । । 7.80 8.00 8.20 8.40 m/z 82.95 11.48% 99 , 127 155 183 211 1’111’112019u01111’1’23-1330113201231121’CuBPUTITT ।■•■ lz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #52385: 1-Hexacosanol 43 ■ ‘ i ' • ‘ 1 i ' 1 1 ' I 7.80 8.00 8.20 8.40 5000 83 m/z 126.85 11.41%

1 111 NAl,....................... 336 364 mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #12247:2-Propanone, 1,1,1 -trichloro- 1 1 ■ i ‘ ■ ■ ■ i • ■ ■ ■ i ■ ■ ■ ‘ i ■ ■ ■ ■ i 43 7.80 8.00 8.20 8.40 m/z 96.90 11.02% 5000

15 mmmpmtn 1 85 125 ugpp miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 7.80 8.00 8.20 8.40

12095.D GCMS0520.M Fri May 31 11:34:39 2002 Page 2

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