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GCMS sample results AE11284, DEP Labs, June 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry results for sample AE11284 analyzed on June 4, 2002.

NYC-WTC_000014781–000014806

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 12 Benzene, 1-ethyl-2,3-dimethyl- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 13.46 0.80 ug/1 46046 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual —1 Benzene, l-ethyl-2,3-dimethyl- 134 C10H14 000933-98-2 80 2 Benzene, l-methyl-4-(1-methyleth... 134 C10H14 000099-87-6 80 3 Benzene, l-methyl-2-(1-methyleth. .. 134 C10H14 000527-84-4 80 4 Benzene, l-methyl-2-(1-methyleth... 134 C10H14 000527-84-4 80 Abundance Scan 1766 (13.455 min): 11284.D (-1760) (-) m/z 119.20 100.00% 1 9

niz-> 5000

■11 “ ■ ■ i 0 41 67 77 1153,yla1184E mupakulop ■ i ■r ■ ■ i111 ‘r11' ■ i" " 10 2) 30 40 50 60 70 80 90 100 110 120 130 140 91 105 134

" 11 ■ . „ NUA. 13.20 13.40 13.60 13.80 m/z 134.10 29.68% Abundance #53590: Benzene, 1-ethyl-2,3-dimethyl- 1' 9

5000 134 13.20 13.40 13.60 13.80 m/z, 41.20 23.23% 239 E F77 91 105 miz-> +21547451,58,s7.,84,4,98-4 127 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 1111 ‘1 ■> I I I I

Abundance #120808: Benzene, 1-methyl-4-(1-methylethyl)- 19

13.20 13.40 13.60 13.80 5000 m/z 77.10 21.72% 91 134 27 34 41 51 58 65 77 *I1WWPTCTTTTTTTTTTTTTTT 103 4 p1 127 , • *11 ‘1 * ‘ I “ niz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #53596: Benzene, 1-methyl-2-(1-methylethyl)- 119 j Li 13.20 13.40 13.60 13.80 m/z 91.10 . 20.80% 5000 134 91 15 27 39 51 58 65 77 84 I Tr 103 -- nieeplagonAYer T 127 ,’ I’’ 1 ■ ■ i ■ 1 A •A• 'I iz—> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 13.20 13.40 13.60 13.80

11284.D SCAN020507.M Fri May 17 13:06:43 2002 Page 15

NYC-WTC_000014797

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NYC-WTC_000014797Source: NYC Law Department, mirrored locally

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