GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************************** * Peak Number 7 Benzene, 1-methyl-4-(1-meth... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 10.01 0.05 ug/L 34603 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, l-methyl-4-(1-methyleth... 134 C10H14 000099-87-6 90 2 Benzene, 1-methyl-4-(1-methyleth... 134 C10H14 000099-87-6 90 3 Benzene, l-methyl-2-(1-methyleth. . . 134 C10H14 000527-84-4 90 4 Benzene, 4-ethyl-l,2-dimethyl- 134 C10H14 000934-80-5 90 Abundance Scan 581 (10.007 min): 28324A.D (-) m/z 119.05 100.00% 1 9

5000

41 77 91 134 .A..N____ 9.60 9.80 10.00 10,20 10,40 I 0 TTUBUIE——.TITT 51 m/z 134.10 29.60% mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29886: Benzene, 1-methyl-4-(1-methylethyl)- (CAS) $$ p-Cy... V9

5000 134 9.60 9.80 10,00 10,20 10,40 91 m/z 91.10 21.74% 66 77 103 0 ■ । ■1 ‘11 • ■' ■ ।1 ■'' । ■ ■ ■ ■ । ■1 ■ ।' ■'' । ' ' 'I 1 N —4+ — mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29890: Benzene, 1-methyl-4-(1 -methylethyl)- (CAS) $$ p-Cy... 1* 9

9.60 9,80 10.00 10.20 10.40 5000 m/z 117.10 17.87% 91 134 27 77 0 TWWITT-TITTT miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29875: Benzene, 1-methyl-2-(1-methylethyl)- (CAS) $$ 1-Me... 19 9.60 9.80 10.00 10,20 10,40 m/z 120.10 13.84% 5000 134 91

m/z-> 0 20 30 40 50 60 65 I 70 77 1 80 L 11100।103'h 1 110 90 . । ।! । । 11 11 11111 120 130 140 9.60 9.80 10.00 10.20 10.40

28324A.D SCAN508.M Fri Feb 22 11:44:12 2002 Page 9

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