GCMS sample results AE12093, DEP Labs, June 2002

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Gas chromatography mass spectrometry results for sample AE12093 analyzed on June 4, 2002.

NYC-WTC_000014764–000014770

Folder label: “GCMS X 5/29/02 A 5/30/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 9

Data File : C:\HPCHEM\1\DATA\MAY2302\12093.D Vial: 8 Acq On : 23 May 2002 7:01 pm Operator: Morgan Sample : 5/21 bn Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 15:47 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table N Last Update : Fri May 31 15:47:14 2002 MP j Response via : Initial Calibration . X J DataAcq Meth : GCMS0520 XN0 _ A

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.14 152 461300 40.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 1678368 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.09 164 914468 40.00 ug/1 0.00 30) Phenanthrene-diO 25.53 188 1198920 40.00 ug/1 0.00 38) Chrysene-dl2 33.59 240 666071 40.00 ug/1 -0.01 44) Perylene-dl2 37.81 264 457862 40.00 ug/1 0.00 System Monitoring Compounds 28) TCMX 23.23 209 127109 27.66 ug/L 0.00 Spiked Amount 40.000 Recovery - <69.15%

Target Compounds alue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77. 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.58 149 239 N.D. 26) 4-Chlorophenylphenylether 23.23 204 454 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.24 168 345 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.53 178 114 N.D. (#) = qualifier out of range (m) = manual integration 12093.D GCMS0520.M Fri May 31 15:47:49 2002 Page 1

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