GCMS blank analysis results, DEP Labs, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY3 0 02\CAL20.D Vial: 17 Acq On 31 May 2002 10:18 am Operator: Morgan Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 11:29 2002 Quant Results File:~GCMS0520.RES

Quant Method : C:\rfPCHEM\l\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 11:29:36 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 520972 40.00 ug/1 -0.08 10) Naphthalene-d8 15.69 136 2080083 40.00 ug/1 -0.10 17) Acenaphthene - dl 0 20.99 164 982528 40.00 ug/1 -0.10 30) Phenanthrene-diO 25.42 188 1528107 40.00 ug/1 -0.11 38) Chrysene-dl2 33.47 240 941719 40.00 ug/1 -0.13 44) Perylene-dl2 37.65 264 613390 40.00 ug/1 -0.15 System Monitoring Compounds 28) TCMX 23.13 209 56992 11.54 ug/L -0.11 Spiked Amount 10.000 Recovery = 115.40% Target Compounds /4>% Qvalue 2) N-nitrosodimethylamine 5.72 74 264024 16.88 ug/1 80 3) bis(2-Chloroethyl)ether 11.47 93 347049 16.75 ug/1 91 4) 1,3-Dichlorobenzene 11.96 146 353852 21.11 ug/1 97 5) 1,4-Dichlorobenzene 12.11 146 382725 20.83 ug/1 100 6) 1,2-Dichlorobenzene 12.63 146 333164 20.93 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.95 45 528390 11.27 ug/1 # 92 8) N-Nitrosodi-n-propylamine 13.33 70 233057 15.84 ug/1 # 85 9) Hexachloroethane 13.47 117 149444 19.05 ug/1 100 11) Nitrobenzene 13.75 77 316416 17.50 ug/1 # 86 12) Isophorone 14.39 82 603362 16.85 ug/1 94 13) bis(2-Chloroethoxy)methane 15.08 93 397425 16.56 ug/1 # 98 14) 1,2,4-Trichlorobenzene 15.58 180 281653 21.68 ug/1 99 15) Naphthalene 15.75 128 952513 20.28 ug/1 # 81 16) Hexachlorobutadiene 16.30 225 123055 19.57 ug/1 100 18) Hexachlorocyclopentadiene 18.49 237 91416 22.94 ug/1 100 19) 2-Chloronaphthalene 19.25 162 452696 20.67 ug/1 97 20) Dimethylphthalate 20.35 163 568697 20.63 ug/1 99 21) 2,6-Dinitrotoluene 20.56 165 119899 20.89 ug/1 93 22) Acenaphthylene 20.52 152 821999 20.49 ug/1 98 2 3) Acenaphthene 21.08 153 492748 20.55 ug/1 99 24) 2,4-Dinitrotoluene 21.72 165 136011 21.62 ug/1 # 87 25) Diethylphthalate 22.48 149 527625 20.71 ug/1 99 26) 4-Chlorophenylphenylether 22.63 204 268056 21.05 ug/1 99 27) Fluorene 22.60 166 527163 21.69 ug/1 100 29) Azobenzene 23.09 77 620989 16.92 ug/L # 90 31) N-Nitrosodiphenylamine 23.02 168 214202 21.27 ug/1 # 87 32) 4-Bromophenylphenylether 24.09 248 135054 16.93 ug/1 96 3 3) Hexachlorobenzene 24.52 284 150739 17.61 ug/1 96 3 4) Phenanthrene 25.49 178 778291 21.12 ug/1 99 (#) = qualifier out of range (m) = manual integration CAL20.D GCMS0520.M Fri May 31 11:30:59 2002 Page 1

NYC-WTC_0000 14743