GCMS blank report, DEP Box 15, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2902\CAL80.D Vial: 2 Acq On : 29 May 2002 12:18 pm Operator: Morgan Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY-P Quant Time: May 29 14:05 2002 Quant Results File: GCMS0528.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 29 14:05:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 706232 40.00 ug/1 -0.07 10) Naphthalene-d8 15.70 136 2858460 40.00 ug/1 -0.09 17) Acenaphthene-diO 21.00 164 1335728 40.00 ug/1 -0.09 30) Phenanthrene-diO 25.43 188 2128006 40.00 ug/1 -0.10 38) Chrysene-dl2 33.49 240 1370549 40.00 ug/1 -0.11 44) Perylene-dl2 37.67 264 895619 40.00 ug/1 -0.13 System Monitoring Compounds 28) TCMX 23.14 209 67937 7.37 ug/L -0.10 Spiked Amount 10.000 Recovery = 73.70% Target Compounds $0//07 Qvalue 2) N-nitrosodimethylamine 5.74 74 1411468 66.58 ug/1 80 3) bis(2-Chloroethyl)ether 11.47 93 1815111 64.63 ug/1 94 4) 1,3-Dichlorobenzene 11.97 146 1777421 78.21 ug/1 100 5) 1,4-Dichlorobenzene 12.11 146 1929187 77.47 ug/1 98 6) 1,2-Dichlorobenzene 12.63 146 1688191 7825 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.96 45 2830128 44.54 g/l 93 8) N-Nitrosodi-n-propylamine 13.35 70 1249865 ug/l # 85 9) Hexachloroethane 13.47 117 758365 71.33 ug/1 96 11) Nitrobenzene 13.75 77 1704485 68.61 ug/1 # 88 12) 1sophorone 14.40 82 3175740 64.55 ug/1 96 13) bis(2-Chloroethoxy)methane 15.09 93 2076075 62.95 ug/1 99 14) 1,2,4-Trichlorobenzene 15.59 180 1400030 78.41 ug/1 99 15) Naphthalene 15.76 128 4775137 73.99 ug/1 # 81 16) Hexachlorobutadiene 16.31 225 619826 71.74 ug/1 100 18) Hexachlorocyclopentadiene 18.49 237 558250 103.06 ug/1 99 19) 2-Chioronaphthalene 19.26 162 2300532 77.27 ug/1 96 20) Dimethylphthalate 20.36 163 2908652 77.62 ug/1 99 21) 2,6-Dinitrotoluene 20.58 165 668043 85.63 ug/1 92 22) Acenaphthylene 20.53 152 4162245 76.30 ug/1 98 23) Acenaphthene 21.10 153 2479099 76.06 ug/1 98 24) 2,4-Dinitrotoluene 21.74 165 785401 91.85 ug/1 # 88 25) Diethylphthalate 22.49 149 2713888 78.37 ug/1 99 26) 4-Chlorophenylphenylether 22.64 204 1297499 74.96 ug/1 99 27) Fluorene 22.61 166 2542766 76.95 ug/1 99 29) Azobenzene 23.11 77 3263031 65.41 ug/L # 91 31) N-Nitrosodiphenylamine 23.04 168 975278 69.55 ug/1 # 86 32) 4-Bromophenylphenylether 24.10 248 682272 61.41 ug/1 93 33) Hexachlorobenzene 24.53 284 746824 62.66 ug/1 # 91 34) Phenanthrene 25.51 178 3794796 73.95 ug/1 100 (#) = qualifier out of range (m) = manual integration CAL80.D GCMS0528.M Wed May 29 14:08:54 2002 Page 1

NYC-WTC_000013784