GCMS calibration table data, sample AE09678, May 2002

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Data File C:\HPCHEM\l\DATA\MAY0602\9678.D Vial: 21 Acq On 7 May 2002 11:53 am Operator: Sample GC/MS SCAN 4/25 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to. I STD R.T.

8.16 11.37 ug/1 985189 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 Acetone? 58 C3H60 000067-64-1 9 3 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 4 5-Hexen-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 341 (8.163 min): 9678.D (-) m/z 43.05 100.00%l 43

5000 59

101 7.80 8.00 8.20 8.40 8.60 miz—> -------38+ 1p 53 , 1—mnmpmmngmmBmRmaTT 69 83 TTHIPpmp 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 m/z 59.10 43.439 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

. ... ....... ..... 5000 59 780 8.00 8.20 8.40 8.60 m/z 58.10 17.169 27 49 . 101 -H . I.।.... ।.... ।. .1.11I ... । ।.... ।.... ।.।83 1’1 iz—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #62322: Acetone 43

7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.889 58 27 mHH+ 1I‘mIUI"u—u—u—uu"unm1—0————3mm m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 m/z 41.15 6.88% 5000

58 72 100 38,+ I ‘" I 11UW-T"TTTITTTTTTTTWT"WTTTTTT m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 — 7.80 8.00 8.20 8.40 8.60

9678.D GCMS0501.M Thu May 09 11:25:29 2002 Page 1

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